Research Notes I, 1949

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HSbCl₆ was prepared by treating chemically pure SbCl₅ with 10% (~3 N) hydrochloric acid, both of the reagents were precooled to the temp of ice water. [left margin]a fuming liquid[/margin]

HSbCl₆ is unstable at room temperatures Signal amplitude was reduced to about 20% after standing for 24 hours.

Suggestion: mean life time of the compound can be measured with the spectrometer.

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